Beam test of a one-dimensional position sensitive chamber on synchrotron radiation

LIU Mei; DAI Hong-Liang; QI Hui-Rong; ZHUANG Bao-An; ZHANG Jian; LIU Rong-Guang; ZHU Qi-Ming; OUYANG Qun; CHEN Yuan-Bo; JIANG Xiao-Shan; WANG Ya-Jie; LIU Peng; CHANG Guang-Cai

doi:10.1088/1674-1137/37/10/108001

Chinese Physics C> 2013, Vol. 37> Issue(10) : 108001 DOI: 10.1088/1674-1137/37/10/108001

Beam test of a one-dimensional position sensitive chamber on synchrotron radiation

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A one-dimensional single-wire chamber was developed to provide high position resolution for powder diffraction experiments with synchrotron radiation. A diffraction test using the sample of SiO₂ has been accomplished at 1W2B laboratory of Beijing Synchrotron Radiation Source. The data of the beam test were analyzed and some diffraction angles were obtained. The experimental results were in good agreement with standard data from ICDD powder diffraction file. The precision of diffraction angles was 1% to 4.7%. Most of the relative errors between measured values of diffraction angles and existing data were less than 1%. As for the detector, the best position resolution in the test was 138 μm (σ value) with an X-ray tube. Finally, discussions of the results were given. The major factor that affected the precision of measurement was deviation from the flat structure of the detector. The effect was analyzed and the conclusion was reached that it would be the optimal measurement scheme when the distance between the powder sample and detector was from 400 mm to 600 mm.

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LIU Mei, DAI Hong-Liang, QI Hui-Rong, ZHUANG Bao-An, ZHANG Jian, LIU Rong-Guang, ZHU Qi-Ming, OUYANG Qun, CHEN Yuan-Bo, JIANG Xiao-Shan, WANG Ya-Jie, LIU Peng and CHANG Guang-Cai. Beam test of a one-dimensional position sensitive chamber on synchrotron radiation[J]. Chinese Physics C, 2013, 37(10): 108001. doi: 10.1088/1674-1137/37/10/108001

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Received: 2012-11-19
Revised: 2012-12-21

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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Beam test of a one-dimensional position sensitive chamber on synchrotron radiation

Corresponding author: LIU Mei,

Corresponding author: QI Hui-Rong,

Received Date: 2012-11-19

Accepted Date: 2012-12-21

Available Online: 2013-10-05

Abstract: A one-dimensional single-wire chamber was developed to provide high position resolution for powder diffraction experiments with synchrotron radiation. A diffraction test using the sample of SiO₂ has been accomplished at 1W2B laboratory of Beijing Synchrotron Radiation Source. The data of the beam test were analyzed and some diffraction angles were obtained. The experimental results were in good agreement with standard data from ICDD powder diffraction file. The precision of diffraction angles was 1% to 4.7%. Most of the relative errors between measured values of diffraction angles and existing data were less than 1%. As for the detector, the best position resolution in the test was 138 μm (σ value) with an X-ray tube. Finally, discussions of the results were given. The major factor that affected the precision of measurement was deviation from the flat structure of the detector. The effect was analyzed and the conclusion was reached that it would be the optimal measurement scheme when the distance between the powder sample and detector was from 400 mm to 600 mm.

Beam test of a one-dimensional position sensitive chamber on synchrotron radiation

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通讯作者: 陈斌, bchen63@163.com

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