High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C3N4

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ZHOU Qiang, HE Zhi, LI Fang-Fei, ZHANG Jian, LI Xue-Fei, MA Yan-Mei, PENG Gang, CUI Qi-Liang, LIU Jing and ZOU Guang-Tian. High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C3N4[J]. Chinese Physics C, 2005, 29(S1): 126-129.
ZHOU Qiang, HE Zhi, LI Fang-Fei, ZHANG Jian, LI Xue-Fei, MA Yan-Mei, PENG Gang, CUI Qi-Liang, LIU Jing and ZOU Guang-Tian. High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C3N4[J]. Chinese Physics C, 2005, 29(S1): 126-129. shu
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Received: 2005-10-31
Revised: 1900-01-01
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High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C3N4

    Corresponding author: CUI Qi-Liang,
  • National Laboratory of Superhard Materials,Jilin University,Changchun 130012,China2 Institute of High Energy Physics,Chinese Academy of Sciences,Beijing 100049,China

Abstract: Pure beta-C3N4 with symmetry group P63/M (176) and cubic C3N4 were synthesized in laser heated diamond anvil cell under high pressure and high temperature conditions. The precise XRD analysis (Rwp=2.8) was successfully performed to refine the structures of graphite C3N4 and beta-C3N4. Moreover, the structural transition from beta-C3N4 to cubic C3N4 was monitored by In-situ high pressure synchrotron X-ray diffraction analysis.

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