Synchrotron X-ray diffraction study of phenacite at high pressure

FAN Da-Wei; MA Mai-Ning; WEI Shu-Yi; CHEN Zhi-Qiang; XIE Hong-Sen

doi:10.1088/1674-1137/36/2/014

Chinese Physics C> 2012, Vol. 36> Issue(2) : 179-183 DOI: 10.1088/1674-1137/36/2/014

Synchrotron X-ray diffraction study of phenacite at high pressure

Abstract
HTML
Reference
Related

PDF

Abstract：
We report the results of a natural phenacite from 0 to 30.9 GPa using in situ angle-dispersive X-ray diffraction and a diamond anvil cell at the National Synchrotron Light Source, Brookhaven National Laboratory. Over this pressure range, no phase change or disproportionation has been observed. The isothermal equation of state was determined. The values of V₀, K₀, and K₀′ refined with a third-order Birch-Murnaghan equation of state are V₀=1116.1±1.2 Å³, K₀=223±9 GPa, and K₀′=5.5±0.8. Furthermore, we confirm that the linear compressibilities (β) along a and c directions of phenacite are elastically isotropic (β_a=1.50×10^-3 and β_c=1.34×10^-3 GPa^-1). Consequently, it can be concluded that the compressibility of phenacite under high pressures has been accurately constrained.

References

[1]

Bragg L, Claringbull G F. Crystal Structure of Minerals.Bell, London, 19652 Zachariasen W H. Soviet Physics Crystallography, 1972,16: 10213 Downs J W. PhD Thesis. Virginia Polytechnic Institutcand State University, Blacksburg, Virginia, 19834 Hazen R M, Au A Y. Physics and Chemistry of Minerals,1986, 13: 695 Yeganeh-Haeri A, Weidner D J. Physics and Chemistry ofMinerals, 1989, 16: 3606 Hazen R M, Finger L W. Physics and Chemistry of Miner-als, 1987, 14: 4267 Gatta G D, Nestola F, Ballaran T B. Physics and Chem-istry of Minerals, 2006, 33: 2358 MAO H K, XU J, Bell P M. Journal of Geophysical Re-search, 1986, 91: 46739 Hammersley J. Fit2d User Manual. ESRF, Grenoble,France, 199610 Holland T J, Tedfern S A. Mineralogical Magazine, 1997,61: 6511 Angel R J. Reviews in Mineralogy and Geochemistry, 2001,41: 3512 Hofmeister A M. Geophysical Research Letters, 1993, 20:635

[1]	Zhen-Jie Li , Yun-Cong Jia , Ling-Fei Hu , Peng Liu , Hua-Xiang Yin . Study of silicon pixel sensor for synchrotron radiation detection. Chinese Physics C, 2016, 40(3): 036001. doi: 10.1088/1674-1137/40/3/036001
[2]	FANG Lei-Ming , CHEN Xi-Ping , SUN Guang-Ai , CHEN Bo , PENG Shu-Ming . Formation of diamond powders from melamine under high pressure and high temperature. Chinese Physics C, 2013, 37(8): 088002. doi: 10.1088/1674-1137/37/8/088002
[3]	ZHANG Yu-Feng , LIU Jing , QIN Zhen-Xing , LIN Chuan-Long , XIONG Lun , LI Rui , BAI Li-Gang . A high-pressure study of PbCO₃ by XRD and Raman spectroscopy. Chinese Physics C, 2013, 37(3): 038001. doi: 10.1088/1674-1137/37/3/038001
[4]	LIU Bo , LIU Ran , LI Quan-Jun , YAO Ming-Guang , ZOU Bo , CUI Tian , LIU Bing-Bing , LIU Jing . Study of high pressure structural stability of CeO₂ nanoparticles. Chinese Physics C, 2013, 37(9): 098003. doi: 10.1088/1674-1137/37/9/098003
[5]	SUN Li-Juan , CUI Ming-Qi , ZHU Jie , ZHAO Yi-Dong , ZHENG Lei , WANG Zhan-Shan , ZHU Jing-Tao . Multilayer-based soft X-ray polarimeter at the Beijing Synchrotron Radiation Facility. Chinese Physics C, 2013, 37(7): 078001. doi: 10.1088/1674-1137/37/7/078001
[6]	DENG Biao , YANG Qun , XIE Hong-Lan , DU Guo-Hao , XIAO Ti-Qiao . First X-ray fluorescence CT experimental results at the SSRF X-ray imaging beamline. Chinese Physics C, 2011, 35(4): 402-404. doi: 10.1088/1674-1137/35/4/015
[7]	LIU Ying-Xin , QIN Shan , WU Xiang , JIANG Jian-Zhong , Kikegawa Takumi , SHI Guang-Hai . High pressure X-ray diffraction study of SrMnO₃ perovskite. Chinese Physics C, 2011, 35(5): 514-518. doi: 10.1088/1674-1137/35/5/022
[8]	TAN Gao , WANG Hua-Qiao , CHEN Yu , YUAN Qing-Xi , LI Gang , ZHANG Xiao-Dan , ZHU Pei-Ping , ZHONG Xiu-Feng , TANG Jin-Tian . X-ray diffraction enhanced imaging study of intraocular tumors in human beings. Chinese Physics C, 2010, 34(2): 237-244. doi: 10.1088/1674-1137/34/2/016
[9]	LAN Ding , WANG Yu-Ren , ZHANG Yin-Min , WANG Wei , WU Zhong-Hua . Small angle X-ray scattering of the colloidal crystal. Chinese Physics C, 2009, 33(11): 1016-1018. doi: 10.1088/1674-1137/33/11/017
[10]	WANG Wen-Xin , ZHANG Yi , WANG Ji-Jin , HU Bi-Tao . Study on spatial resolution of micromegas as a neutron detector under condition of high neutron flux and γ ray background. Chinese Physics C, 2009, 33(2): 110-113. doi: 10.1088/1674-1137/33/2/007
[11]	TANG Chuan-Xiang , LI Ren-Kai , HUANG Wen-Hui , CHEN Huai-Bi , DU Ying-Chao , DU Qiang , DU Tai-Bin , HE Xiao-Zhong , HUA Jian-Fei , LIN Yu-Zhen , QIAN Hou-Jun , SHI Jia-Ru , XIANG Dao , YAN Li-Xin , YU Pei-Cheng . A simulation study of Tsinghua Thomson scattering X-ray source. Chinese Physics C, 2009, 33(S2): 146-150. doi: 10.1088/1674-1137/33/S2/038
[12]	ZHAI Zhang-Yin , WU Xiao-Shan , JIA Quan-Jie . High resolution X-ray diffraction investigation of epitaxially grown SrTiO₃ thin films by laser-MBE. Chinese Physics C, 2009, 33(11): 949-953. doi: 10.1088/1674-1137/33/11/004
[13]	XU Tao , HUANG Lei , DONG Yan-Guo , LI Gong , LI Yan-Chun , LIU Jing , LIU Ri-Ping . In situ X-ray diffraction investigation of compression behavior in Gd₄₀Y₁₆Al₂₄Co₂₀ bulk metallic glass under high pressure with synchrotronradiation. Chinese Physics C, 2009, 33(11): 1028-1032. doi: 10.1088/1674-1137/33/11/020
[14]	HUA Zheng-Dong , XU Xun-Jiang , WANG Jian-Hua , LIU Shu-Dong , LI Jian-Ping . Study of the energy response of high pressure ionization chamber for high energy gamma-ray. Chinese Physics C, 2008, 32(5): 370-372. doi: 10.1088/1674-1137/32/5/008
[15]	LUO Cong-Ju , LIU Jing , XU Ji-An , XIAO Wan-Sheng , LI Hui , LI Xiao-Dong . Energy Dispersive X-Ray Diffraction Investigation of Beryllium Oxide under High Pressure. Chinese Physics C, 2005, 29(S1): 106-108.
[16]	TANG Ling-Yun , LIU Jing , XIAO Wan-Sheng . High Pressure X-Ray Diffraction of SrF₂. Chinese Physics C, 2005, 29(S1): 109-111.
[17]	ZHOU Qiang , HE Zhi , LI Fang-Fei , ZHANG Jian , LI Xue-Fei , MA Yan-Mei , PENG Gang , CUI Qi-Liang , LIU Jing , ZOU Guang-Tian . High-Temperature High-Pressure Synchrotron X-Ray Diffraction Study of C₃N₄. Chinese Physics C, 2005, 29(S1): 126-129.
[18]	YU Zhi-Wu , FENG Ying , WANG Jun , DONG Bao-Zhong . Study of the Effect of Urea on the Phase Transition of Phospholipid by Synchrotron X-Ray Diffraction. Chinese Physics C, 2001, 25(S1): 75-80.
[19]	Wang Jun , Cui Mingqi , Xu Wenxuan , Huang Yuying , Wang Dewu , Liu Jianfei , Xian Dingchang . Study of Multilayer Structures by Synchrotron Radiation with Small Angle Diffraction Method. Chinese Physics C, 1993, 17(S4): 311-319.
[20]	Zhao Jivong , Yang Ping , Jiang Jianhua , Tian Yulian , Han Yong , Wang Chunxi , Shi Caitu , Xian Dingchang . Light Source for Synchrotron Radiation Topographical Study at Beijing Synchrotron Radiation Facility (BSRF). Chinese Physics C, 1992, 16(S3): 235-241.

Access

Get Citation

FAN Da-Wei, MA Mai-Ning, WEI Shu-Yi, CHEN Zhi-Qiang and XIE Hong-Sen. Synchrotron X-ray diffraction study of phenacite at high pressure[J]. Chinese Physics C, 2012, 36(2): 179-183. doi: 10.1088/1674-1137/36/2/014

RIS(for EndNote,Reference Manager,ProCite)

BibTex

Txt

Milestone

Received: 2011-04-26
Revised: 2011-06-08

Article Metric

Article Views(2356)
PDF Downloads(377)
Cited by(0)

Policy on re-use

To reuse of subscription content published by CPC, the users need to request permission from CPC, unless the content was published under an Open Access license which automatically permits that type of reuse.

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Synchrotron X-ray diffraction study of phenacite at high pressure

Corresponding author: FAN Da-Wei,

Corresponding author: MA Mai-Ning,

Received Date: 2011-04-26

Accepted Date: 2011-06-08

Available Online: 2012-02-05

Abstract: We report the results of a natural phenacite from 0 to 30.9 GPa using in situ angle-dispersive X-ray diffraction and a diamond anvil cell at the National Synchrotron Light Source, Brookhaven National Laboratory. Over this pressure range, no phase change or disproportionation has been observed. The isothermal equation of state was determined. The values of V₀, K₀, and K₀′ refined with a third-order Birch-Murnaghan equation of state are V₀=1116.1±1.2 Å³, K₀=223±9 GPa, and K₀′=5.5±0.8. Furthermore, we confirm that the linear compressibilities (β) along a and c directions of phenacite are elastically isotropic (β_a=1.50×10^-3 and β_c=1.34×10^-3 GPa^-1). Consequently, it can be concluded that the compressibility of phenacite under high pressures has been accurately constrained.

HTML

Reference (1)

Synchrotron X-ray diffraction study of phenacite at high pressure

Abstract：

References

Access

Article Metrics

Metrics

通讯作者: 陈斌, bchen63@163.com

Email This Article